Reduction of thermally grown single-phase CuO and Cu2O thin films by in-situ time-resolved XRD

نویسندگان

چکیده

Copper oxide is used as a catalyst or precursor in chemical reactions that involve hydrogen reactant product. Controlled reduction and therefore known kinetics of well-defined Cu-oxides key issue for the activation catalysts well other technological fields such gas sensing. The mechanisms single-phase CuO Cu2O films 5 vol% H2/Ar were investigated by in-situ real time synchrotron-based X-ray diffraction measurements. To this end, incubation time, → Cu phase transformation rates, microstructure strain state evolving Cu, phases studied during reduction. Highly porous scaffolds obtained alternating oxidation steps, which can be envisaged wealth applications catalysis, batteries, water treatment biomedical applications.

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ژورنال

عنوان ژورنال: Applied Surface Science

سال: 2022

ISSN: ['1873-5584', '0169-4332']

DOI: https://doi.org/10.1016/j.apsusc.2022.152896